"ERRATIC LASER SIGNAL" ON OLDER PERKIN-ELMER FTIR,
RX-1 & 1600
SYMPTOM: during power-up, the test program gives an ERRATIC LASER SIGNAL error. Low laser signal
is usually responsible, and the cause can be: laser's drifting
mechanical alignment, aging laser tube or HV power supply, or even humidity-damaged KBr in the
windows or beamsplitter.
See Youtube vid from Tesla500: Perkin Elmer 1600 teardown
These old FTIR units employ an actual HeNe laser tube as their interferometer geometry reference.
Old-school technology. "Vintage." But replacements still available from Perkin-Elmer for the Spectrum RX1,
or direct from Melles-Griot for the Model 1600, see below.
TEST: inside the instrument sample well, verify red output beam by holding a white card in the well
when the instrument is up and running. (Switch out the energy probe assy, or just remove it from
the well.) Note the small red dot; usually somewhat dim in normal room lighting, but *not*
near-invisible. The beam comes in from the left side of the well.
If a dim red spot is absent in the well, open the instrument case, pull up the
interlock switch to apply power, and after the laser tube lights up pink, hold a
white card in the gap between the right end of the laser housing and the plastic
opto-bench cover. When working correctly, the beam should appear as a piercingly-
intense red dot, similar to a 1mW red laser pointer. If the beam is dim or
absent, either the kilovolt laser supply has failed, or the 12VDC to the laser supply is
missing, or perhaps it may be time for a new laser tube. (With the housing open, does
the laser tube have some blue plasma, or distinct purple highlights around the pink
glow? If so, then it's "gassy," and N2/O2 has got through the seals.
Over years of operation
these gas-discharge tubes always degrade and eventually fail. Nitrogen slowly leaks in through the seals
for the laser mirrors, while Helium slowly becomes "gettered" by the laser's metal electrodes. Eventually
the tube's output milliwatts drops too low to run the unit's interferometer. In this case the tube will either
stop lasing entirely, that or the direct output will be a dim red spot on a white card. During such old-age
tube failure, in the PE 1600 you'll still see a bright glow in the laser tube. With the RX-1, if you release
the springs and lift the working tube from its bracket, you should still see a pink or violet glow down inside
the output orfice. In either case, a bright blue/violet glow can indicate N2/O2 in the gas mix.
If the laser's output beam is still there and plenty bright, then probably the laser tube is just
misaligned. This is a fairly common failure, since over several years, any slight vibration of your
lab bench can wiggle
the laser around in its bracket. The laser bracket has an X/Y adjustment via long 3/32" hex-wrench accessible
through two holes in the top of the laser box. While in test-mode, use
a hex driver to maximize the laser reading. Note that sometimes the X/Y adjustment isn't enough,
and a working-but-old laser tube
must be rotated or shimmed to give best aim. The beam both must strike that tiny 3mm mirror-chip on
the optical bench, but also it must follow the entire IR path to reach the
visible-light detector at the end. Sometimes the hex-nut X/Y adjustments don't attain the actual maximum
available, but trimming the laser tube can do it.
Much more rarely the kilovolt tube-driver supply will fail. In this case there will be no red output
beam, but also the PE-1600 laser tube remains dark, and for the RX-1, no glow is seen when looking into
the laser output orfice.
PARTS:
L1181245 laser module for Spectrum RX1 FTIR, enclosed HeNe tube,
approx $2000 (in 2013) [order from PE field service]
3121H-P-02-73 HeNe laser tube for 1600 FTIR, bare tube, Melles-Griot, approx $650 (in 2012)
800-645-2737 x3115 [INSURE FOR FULL VALUE, or ups will run a forklift tire over the box.]
Also, here's a KBr beamsplitter refurbish service,
and an FTIR parts/repair service w/lasers, but I've not yet tried either one.
LASER GAIN ADJUST, RX-1, PRESS THE FOLLOWING CONSOLE BUTTONS
[SETUP]
[OTHERS] <-- note, not the adjacent [EXIT] button
[OTHERS]
[TEST]
[ADJUST]
[LASER]
In laser-adjust mode, just press [AUTO] and the system should adjust its gain for proper operation.
Repeatedly press [CANCEL] to back out of this mode.
See also:
- Perkin-Elmer FTIR, using a USB printer
- Perkin-Elmer FTIR source IR fails